Re sebelisa li-cookies ho ntlafatsa boiphihlelo ba hau.Ka ho tsoela pele ho sheba sebaka sena sa marang-rang, o lumellana le ts'ebeliso ea rona ea li-cookies.Tlhahisoleseling e 'Ngoe.
Batho lefatšeng ka bophara ba sebelisa lino-mapholi ho ntlafatsa maikutlo le tlhahiso ea bona.E 'ngoe ea litsela tse atlehang ka ho fetisisa tsa ho hlahloba lino tsena ke capillary electrophoresis.Sengoliloeng sena se hlahloba bokhoni le bohlokoa ha se bapisoa le mekhoa e meng joalo ka mokelikeli oa chromatography.
Bongata ba lino tse matla li entsoe ka metsoako e nang le caffeine e ngata, ho akarelletsa le caffeine le glutamate.Caffeine ke alkaloid e susumetsang e fumanoang mefuteng e fetang 63 ea limela lefatšeng ka bophara.Kafeine e hloekileng ke ntho e babang, e sa latsoeheng, e tšoeu e tiileng.Boima ba molek'hule ea caffeine ke 194.19 g, ntlha e qhibilihang ke 2360°C.K'hafeine e na le hydrophilic mocheso oa kamore 'me e fihla ho 21.7 g/l ka lebaka la ts'ebetso ea eona e itekanetseng.
Linoa-mapholi ke litsamaiso tse rarahaneng tse nang le metsoako e mengata e fapaneng, ka bobeli le li-organic.Licheke tsa karohano li bohlokoa ho fumana le ho lekola mefuta e meng e fapaneng ea caffeine le benzoate.Mokhoa o sebelisoang haholo ho lekola likarohano tse kopaneng ke liquid chromatography (LC).
Liquid chromatography e tlalehoa e sebelisoa ho khetholla pakeng tsa mefuta e mengata ea limolek'hule tsa tlhaho, ho tloha ho litšila tse nyenyane tsa boima ba limolek'hule ho ea ho li-peptide tse thibelang likokoana-hloko.Likhokahano tse fapaneng lipakeng tsa mekhahlelo e tsamaeang le e emeng ea limolek'hule ka har'a sampole li theha karohano ea mokelikeli oa chromatography.Ha maqhama a ntse a le matla, molek'hule e tla ba le boemo ba eona hantle.
Mokhoa o mong ho fapana le lits'ebetso tsa HPLC ke karohano ka moqotetsane bore fused silica capillary electrophoresis, e sebelisang lebala la motlakase ho arola metsoako ho tsoa ho lihlopha tse fapaneng tsa lik'hemik'hale sampoleng e le 'ngoe.CE e ka aroloa ka mekhoa e mengata ea karohano ho latela li-capillaries le li-ion tse sebelisitsoeng.
Mokhoa oa capillary electrophoresis o thusa haholo bakeng sa tlhahlobo ea lijo le seno ka lebaka la melemo ea eona ea sampole e tlase le tšebeliso ea reagent, nako e khuts'oane ea tlhahlobo, litšenyehelo tse tlase tsa ts'ebetso, tharollo e phahameng, ts'ebetso e phahameng ea ho tlosa, bonolo ba liteko le nts'etsopele ea ts'ebetso e potlakileng.
Mokhoa oa ho arohana ha electrophoresis o thehiloe metsamaong e fapaneng ea li-ion tsa lik'hemik'hale ka seleng ea electrolytic tlas'a ts'ebetso ea sebaka sa motlakase se sebelisitsoeng.Ha ho bapisoa le lisebelisoa tse rarahaneng tsa chromatography ea mokelikeli, lisebelisoa tsa capillary electrophoresis li bonolo haholo.Pipe e kopanyang e nang le bophara ba ka hare ba 25-100 m le bolelele ba 20-100 cm e hokahanya lisele tse peli tsa buffer, moo matla a phahameng a matla (0-30 kV) a fanoang ka li-conductors 'me potoloho e sebetsang hantle ea electrolysis e kenngoa e le mojari ea qosoang.
Ka tloaelo, anode e nkoa e le capillary inlet 'me cathode e nkoa e le sebaka sa capillary.Palo e nyane ea sampole e kenngoa ka hydraulically kapa ka motlakase ka lehlakoreng la anode ea capillary.Infusion ea motorized e etsoa ka ho fetola sebaka sa polokelo ea polokelo ka sampuli ea vial le ho sebelisa motlakase ka nako e itseng ho lumella likaroloana ho kena ka har'a capillary.
Infusion ea Hydrostatic e fana ka sampole e ipapisitse le ho theoha ha khatello lipakeng tsa ho kena le ho tsoa ha capillary, mme palo ea sampole e kentsoeng e khethoa ke ho theoha ha khatello le botenya ba polymer matrix.Ka mor'a hore sampuli e kenngoe, karolo e 'ngoe ea sampuli e bokellana ho buleha ha capillary.
Thepa ea karohano ea mekhoa ea capillary electrophoresis e ka lekanyetsoa ka litsela tse peli: tharollo ea karohano, Rs, le katleho ea karohano.Qeto ea bahlahlobisisi ba babeli e bontša kamoo ba ka khethollanang ka katleho kateng.Ha boleng ba Rs bo le boholo, tlhoro e itseng e bonahala haholoanyane.Qeto ea karohano e lekanya katleho ea karohano mme e lekola hore na liphetoho tikolohong ea liteko li ka fella ka karohano ea metsoako.
Karohano e sebetsang hantle N ke sebaka se inahaneloang moo mekhahlelo e 'meli e leng ho lekana, e emeloang ke liphanele tse ngata tse fapaneng, ho latela boleng ba kholomo le mokelikeli.
Phuputso e ncha e hatisitsoeng Sebokeng sa Machaba sa Temo le Ts'ebetsong e ikemiselitse ho batlisisa bokhoni ba capillary electrophoresis ho khetholla metsoako ea nitrogenous le ascorbic acid ka lino tse tahang, hammoho le phello ea mefuta-futa ea electrophoresis ka thepa ea bongata ba mokhoa.
Melemo ea capillary electrophoresis holim'a ts'ebetso e phahameng ea mokelikeli chromatography e kenyelletsa litšenyehelo tse tlase tsa lipatlisiso le ho lumellana ha tikoloho, hammoho le tlhahlobo ea asymmetric organic acid kapa litlhōrō tsa motheo.Capillary electrophoresis e fana ka ho nepahala ho lekaneng bakeng sa ho khetholla lik'hemik'hale tsa labile ka matrices a rarahaneng a nang le litekanyetso tse ling tsa motheo (ho hasana ha hlama ka har'a buffer e tsamaeang, ho netefatsa hore homogeneity ea sebopeho sa buffer, ho tsitsisa ha mocheso oa likarolo tse arohaneng).
Ka kakaretso, leha capillary electrophoresis e na le melemo e mengata ho feta chromatography ea mokelikeli o phahameng oa ts'ebetso, e boetse e na le mefokolo joalo ka linako tse telele tsa tlhahlobo.Lipatlisiso tse ling li lokela ho etsoa ho fumana litsela tsa ho ntlafatsa mokhoa ona.
Rashid, SA, Abdulla, SM, Najeeb, BH, Hamarashid, SH, & Abdulla, OA (2021). Rashid, SA, Abdulla, SM, Najeeb, BH, Hamarashid, SH, & Abdulla, OA (2021).Rashid, SA, Abdullah, SM, Najib, BH, Hamarasheed, SH, le Abdullah, OA (2021).Rashid SA, Abdullah SM, Najib BH, Hamarasheed SH le Abdulla OA (2021).Boikemisetso ba caffeine le sodium benzoate ho lino tse tsoang kantle ho naha le tsa lehae tse sebelisang HPLC le spectrophotometer.Letoto la Seboka sa IOP: Lefatše le Saense ea Tikoloho.E fumaneha ho: https://iopscience.iop.org/article/10.1088/1755-1315/910/1/012129/meta.
ALVES, AC, MEINHART, AD, & FILHO, JT (2019). ALVES, AC, MEINHART, AD, & FILHO, JT (2019).ALVES, AS, MEINHART, AD, le FILHO, JT (2019).ALVES, AS, MEINHART, AD le FILHO, JT (2019).Nts'etsopele ea mokhoa oa tlhahlobo ea nako e le 'ngoe ea caffeine le taurine ka matla.Saense ea Lijo le Theknoloji.E fumaneha ho: https://www.scielo.br/j/cta/a/7n534rVddj3rXJ89gzJLXvh/?lang=en
Tuma, Piotr, Frantisek Opekar, le Pavel Dlouhy.(2021).Capillary le microarray electrophoresis e nang le boikemisetso ba ho se kopane le conductivity bakeng sa tlhahlobo ea lijo le seno.k'hemistri ea lijo.131858. E fumaneha ho: https://linkinghub.elsevier.com/retrieve/pii/S0308814621028648.
Khasanov, VV, Slizhov, YG, & Khasanov, VV (2013). Khasanov, VV, Slizhov, YG, & Khasanov, VV (2013).Khasanov VV, Slizhov Yu.G., Khasanov VV (2013).Khasanov VV, Slizhov Yu.G., Khasanov VV (2013).Tlhahlobo ea lino tse matla ka capillary electrophoresis.Journal of Analytical Chemistry.E fumaneha ho: https://link.springer.com/article/10.1134/S1061934813040047.
Fan, KK (207).Tlhahlobo ea capillary ea li-preservatives ho lino tse matla.Univesithi ea California Polytechnic State, Pomona.E fumaneha ho: https://scholarworks.calstate.edu/concern/theses/mc87ps371.
Boitlhotlhollo: Maikutlo a hlahisitsoeng mona ke a sengoli ka boemo ba hae, 'me ha a hlile ha a bontše maikutlo a AZoM.com Limited T/A AZoNetwork, mong'a sebaka sena sa marang-rang.Tlhaloso ena ke karolo ea lipehelo tsa tšebeliso ea sebaka sena sa marang-rang.
Ibtisam o alohile ho Islamabad Institute of Space Technology ka lengolo la bachelor ho boenjiniere ba lifofane.Nakong ea mosebetsi oa hae oa thuto, o 'nile a kenya letsoho mererong e mengata ea ho etsa lipatlisiso 'me o atlehile ho hlophisa mesebetsi e mengata ea ka ntle ho thuto e kang International World Space Week le Seboka sa Machaba sa Boenjiniere ba Aerospace.Ibtisam o hapile tlholisano ea moqoqo oa puo ea Senyesemane matsatsing a hae a seithuti mme esale a bontša thahasello e kholo lipatlisisong, ho ngola le ho hlophisa.Nakoana ka mor'a ho fumana mangolo, o ile a ikopanya le AzoNetwork e le mosebetsi oa boipheliso ho ntlafatsa tsebo ea hae.Ibtisam o rata ho tsamaea, haholo-holo mahaeng.Haesale e le morati wa dipapadi mme a thabela ho shebella tenese, bolo ya maoto le krikete.O hlahetse Pakistan, Ibtisam o tšepa hore ka letsatsi le leng o tla etela lefatše.
Abbasi, Ibtisam.(La 4 Mmesa, 2022).Tlhahlobo ea lino tse matla ka capillary electrophoresis.AZOM.E tsositsoe ka la 13 Mphalane 2022 ho tsoa ho https://www.azom.com/article.aspx?ArticleID=21527.
Abbasi, Ibtisam."Analysis of Energy Drinks by Capillary Electrophoresis".AZOM.La 13 Mphalane, 2022.La 13 Mphalane, 2022.
Abbasi, Ibtisam."Analysis of Energy Drinks by Capillary Electrophoresis".AZOM.https://www.azom.com/article.aspx?ArticleID=21527.(Ho tloha ka la 13 Mphalane 2022).
Abbasi, Ibtisam.2022. Tlhahlobo ea lino tse matla ka capillary electrophoresis.AZoM, e fihletsoe ka la 13 Mphalane 2022, https://www.azom.com/article.aspx?ArticleID=21527.
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Ka lebaka la tlhokahalo e ntseng e hola ea matla, tlhokahalo ea mafura a nyutlelie le eona ea eketseha, e leng se lebisang keketsehong e kholo ea tlhoko ea theknoloji ea tlhahlobo ea morao-rao (PVI).